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Please use this identifier to cite or link to this item: http://hdl.handle.net/1942/22696

Title: Fully quantitative description of hybrid TiO2 nanoparticles by means of solid state P-31 NMR
Authors: Tassi, Marco
Reekmans, Gunter
Carleer, Robert
Adriaensens, Peter
Issue Date: 2016
Publisher: ACADEMIC PRESS INC ELSEVIER SCIENCE
Citation: SOLID STATE NUCLEAR MAGNETIC RESONANCE, 78, p. 50-55
Abstract: For the first time, an absolute quantification of hybrid materials obtained from the reaction of phenylphosphonic acid (PPA) with TiO2 nanoparticles under different reaction conditions is reported. Next to the amount of PPA involved in grafting to the TiO2 nanoparticles, also the PPA included in titaniumphenylphosphonate crystallites is described quantitatively. The quantitative analysis is based on solid state P-31 MAS NMR and is further applied to evaluate the stability of the resulting hybrid materials towards hydrolysis and organic solvent exposure. (C) 2016 Elsevier Inc. All rights reserved.
Notes: [Tassi, Marco; Reekmans, Gunter; Carleer, Robert; Adriaensens, Peter] Hasselt Univ, Inst Mat Res IMO, Appl & Analyt Chem, Agoralaan 1 Bldg D, B-3590 Diepenbeek, Belgium.
URI: http://hdl.handle.net/1942/22696
DOI: 10.1016/j.ssnmr.2016.07.001
ISI #: 000384518300009
ISSN: 0926-2040
Category: A1
Type: Journal Contribution
Validation: ecoom, 2017
Appears in Collections: Research publications

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